6HQ0
Crystal structure of ENL (MLLT1), apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-21 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97950 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 49.419, 49.419, 128.310 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.180 - 1.810 |
R-factor | 0.19369 |
Rwork | 0.192 |
R-free | 0.23661 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5j9s |
RMSD bond length | 0.015 |
RMSD bond angle | 1.459 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0232) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.120 | 1.840 |
High resolution limit [Å] | 1.810 | 1.810 |
Rmerge | 0.090 | 0.841 |
Rpim | 0.028 | 0.286 |
Number of reflections | 15436 | 895 |
<I/σ(I)> | 14.3 | 3.2 |
Completeness [%] | 100.0 | 99.8 |
Redundancy | 11.9 | 10.2 |
CC(1/2) | 0.998 | 0.768 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 30% PEG 2000MME, 0.1M KBr |