6HP8
Crystal structure of DPP8 in complex with Val-BoroPro
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-12-11 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 0.99992 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 163.163, 245.317, 261.588 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 44.620 - 2.500 |
| R-factor | 0.20463 |
| Rwork | 0.203 |
| R-free | 0.22785 |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.916 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (7.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.620 | 2.560 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Rmeas | 0.145 | 1.560 |
| Number of reflections | 179844 | |
| <I/σ(I)> | 15.64 | |
| Completeness [%] | 99.9 | 99.6 |
| Redundancy | 8.4 | 8.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 6.75 | 293 | 0.46 M Na-citrate |
