6HGO
Crystal Structure of human IL-17F
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-04-08 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.99985 |
Spacegroup name | P 65 |
Unit cell lengths | 126.195, 126.195, 88.539 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 63.100 - 2.100 |
R-factor | 0.2 |
Rwork | 0.199 |
R-free | 0.22000 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1jpy |
RMSD bond length | 0.010 |
RMSD bond angle | 1.120 |
Data reduction software | XDS (Sept. 26, 2012) |
Data scaling software | XSCALE (July 4, 2012) |
Phasing software | BUSTER |
Refinement software | BUSTER (2.11.7) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 63.100 | 63.100 | 2.150 |
High resolution limit [Å] | 2.100 | 9.390 | 2.100 |
Rmerge | 0.078 | 0.023 | 1.413 |
Rmeas | 0.082 | 0.024 | 1.488 |
Total number of observations | 477335 | ||
Number of reflections | 46829 | 559 | 3421 |
<I/σ(I)> | 18.6 | 64.33 | 1.66 |
Completeness [%] | 100.0 | 99.6 | 100 |
Redundancy | 10.193 | 10.075 | 10.117 |
CC(1/2) | 0.999 | 0.999 | 0.603 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | 200mM ammonium sulfate, 20.0% PEG 3350 |