6HA7
Crystal structure of the BiP NBD and MANF complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-09-22 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.916 |
Spacegroup name | P 1 |
Unit cell lengths | 58.420, 60.960, 96.110 |
Unit cell angles | 81.13, 88.33, 74.33 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.520 | 2.550 |
High resolution limit [Å] | 2.490 | 2.490 |
Rmerge | 0.050 | 0.707 |
Rmeas | 0.072 | 0.999 |
Rpim | 0.050 | 0.707 |
Number of reflections | 43348 | 3227 |
<I/σ(I)> | 13.3 | 1.6 |
Completeness [%] | 98.1 | 98.1 |
Redundancy | 3.5 | 3.6 |
CC(1/2) | 0.999 | 0.617 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 7% PEG6000, 0.1 M Tris-HCl pH7.5 |