6GVN
Tubulin:TM-3 DARPin complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-1 |
Synchrotron site | ESRF |
Beamline | MASSIF-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-05-04 |
Detector | DECTRIS PILATUS3 2M |
Wavelength(s) | 0.966 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 73.100, 84.260, 81.980 |
Unit cell angles | 90.00, 99.00, 90.00 |
Refinement procedure
Resolution | 43.080 - 2.690 |
R-factor | 0.194 |
Rwork | 0.193 |
R-free | 0.21600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5eyp |
RMSD bond length | 0.010 |
RMSD bond angle | 1.150 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.080 | 2.789 |
High resolution limit [Å] | 2.690 | 2.692 |
Number of reflections | 26956 | |
<I/σ(I)> | 6.22 | |
Completeness [%] | 98.3 | |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG5000 MME, 0.1 M Mes pH 6.0, 150 mM AMMONIUM SULFATE |