6GRO
Human CSNK1G3 bound to SB-223133
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-03-03 |
Detector | DECTRIS PILATUS3 R CdTe 300K |
Wavelength(s) | 0.9763 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 56.750, 56.750, 221.550 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.980 - 1.450 |
R-factor | 0.13503 |
Rwork | 0.134 |
R-free | 0.16732 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2izr |
RMSD bond length | 0.009 |
RMSD bond angle | 1.413 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0222) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.150 | 1.480 |
High resolution limit [Å] | 1.450 | 1.450 |
Rmerge | 0.140 | |
Number of reflections | 74333 | 3637 |
<I/σ(I)> | 6.2 | 2.2 |
Completeness [%] | 99.6 | 98 |
Redundancy | 4.4 | 4.2 |
CC(1/2) | 0.975 | 0.617 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 277 | 0.2 M sodium/potassium tartrate, 0.1 M bis-tris-propane pH 8.5, 20% PEG3350, 10% ethylene glycol |