6GQ7
PI3Kg IN COMPLEX WITH INH
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-08-31 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.972 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 139.590, 67.066, 104.897 |
Unit cell angles | 90.00, 97.28, 90.00 |
Refinement procedure
Resolution | 53.510 - 2.840 |
R-factor | 0.2383 |
Rwork | 0.235 |
R-free | 0.29570 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | Internal model |
RMSD bond length | 0.009 |
RMSD bond angle | 1.080 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Refinement software | BUSTER-TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 61.334 | 2.847 |
High resolution limit [Å] | 2.838 | 2.838 |
Rmerge | 0.087 | 1.352 |
Number of reflections | 22591 | 236 |
<I/σ(I)> | 10.7 | 1.2 |
Completeness [%] | 98.0 | 97.9 |
Redundancy | 3.3 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 20% PEG3350, 175 mM AmSO4, 10 mM DTT and 100 mM Hepes |