6GKT
X-ray structure of a non-autocrystallizing galectin-10 variant, Gal10-Tyr69Glu
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-12-10 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.99998 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 72.823, 93.296, 93.068 |
Unit cell angles | 90.00, 108.94, 90.00 |
Refinement procedure
Resolution | 42.000 - 2.100 |
R-factor | 0.174 |
Rwork | 0.172 |
R-free | 0.20400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1lcl |
RMSD bond length | 0.010 |
RMSD bond angle | 1.120 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.230 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmeas | 0.150 | 2.270 |
Number of reflections | 68207 | 10924 |
<I/σ(I)> | 9.33 | 0.7 |
Completeness [%] | 99.0 | 98.6 |
Redundancy | 6.9 | 6.7 |
CC(1/2) | 0.990 | 0.360 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.2 M ammonium citrate pH 5.1 20% PEG 3350 |