6GFK
delta-N METTL16 MTase domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-08-24 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 133.768, 133.768, 78.701 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 31.950 - 2.300 |
R-factor | 0.196 |
Rwork | 0.195 |
R-free | 0.22800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2h00 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.040 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.32) |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.000 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.059 | 0.721 |
Rmeas | 0.070 | 1.030 |
Rpim | 0.037 | 0.550 |
Number of reflections | 36074 | 3538 |
<I/σ(I)> | 10.3 | 1.4 |
Completeness [%] | 99.4 | 99.6 |
Redundancy | 3.3 | 3.3 |
CC(1/2) | 0.994 | 0.996 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 293 | 1.7M Ammonium Sulfate, 0.2M K/Na Tartrate, 0.1M Na Citrate |