6GE5
TEAD4 (216-434);Y429F COMPLEXED WITH YAP PEPTIDE (60-100) AND MYRISTOATE (COVALENTLY BOUND) AT 2.05A (P41212 CRYSTAL FORM); MYRISTOYLATION WAS DONE BY ADDING MYR-COA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-09-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.99994 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 58.952, 58.952, 159.756 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.500 - 2.050 |
R-factor | 0.2234 |
Rwork | 0.223 |
R-free | 0.23800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ge3 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.964 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.500 | 2.100 |
High resolution limit [Å] | 2.050 | 2.050 |
Rmerge | 0.119 | 0.863 |
Rmeas | 0.124 | 0.898 |
Total number of observations | 237255 | |
Number of reflections | 18467 | |
<I/σ(I)> | 20 | 3.6 |
Completeness [%] | 99.8 | 100 |
Redundancy | 12.8 | 12.8 |
CC(1/2) | 0.999 | 0.881 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4 | 298 | 20% PEG 3350, 8% Tacsimate |