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6G5Y

The X-ray structure of the adduct formed in the reaction between lysozyme and a platinum(II) terpyridine compound (acid pH)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE MASSIF-3
Synchrotron siteESRF
BeamlineMASSIF-3
Temperature [K]100
Detector technologyPIXEL
Collection date2016-10-22
DetectorDECTRIS PILATUS3 2M
Wavelength(s)0.96771
Spacegroup nameP 43 21 2
Unit cell lengths78.490, 78.490, 36.730
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution55.500 - 1.490
R-factor0.19566
Rwork0.193
R-free0.24002
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.018
RMSD bond angle2.078
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0158)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]55.5101.570
High resolution limit [Å]1.4901.490
Rmerge0.0390.514
Rpim0.0250.219
Number of reflections18842
<I/σ(I)>18.13.1
Completeness [%]98.3100
Redundancy3.73.7
CC(1/2)1.0000.672
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP4.428320% ethylene glicol, 0.10 M sodium acetate pH 4.4, 0.60 M sodium nitrate

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