6FZX

LasB, hydroxymate Inhibitor Complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID29
Synchrotron site	ESRF
Beamline	ID29
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-04-20
Detector	DECTRIS PILATUS 6M-F
Wavelength(s)	1.7380
Spacegroup name	P 21 21 21
Unit cell lengths	43.727, 52.982, 122.519
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	61.260 - 2.100
R-factor	0.1808
Rwork	0.179
R-free	0.21320
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1ezm
RMSD bond length	0.003
RMSD bond angle	0.525
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	61.260	2.175
High resolution limit [Å]	2.100	2.100
Rmerge	0.111	0.307
Number of reflections	16581
<I/σ(I)>	4.46
Completeness [%]	95.9
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION		291	1.8 M AMSO4 and 0.1 M Tris-Cl, pH 8.8