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6FZT

Crystal structure of Smad8_9-MH1 bound to the GGCGC site.

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE MASSIF-3
Synchrotron siteESRF
BeamlineMASSIF-3
Temperature [K]100
Detector technologyPIXEL
Collection date2017-12-04
DetectorDECTRIS EIGER X 4M
Wavelength(s)0.967
Spacegroup nameP 21 21 21
Unit cell lengths75.433, 79.509, 88.372
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution59.110 - 2.460
R-factor0.195
Rwork0.193
R-free0.23700
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)6fzs
RMSD bond length0.010
RMSD bond angle1.040
Data reduction softwareXDS
Data scaling softwareautoPROC
Phasing softwarePHASER
Refinement softwareBUSTER (2.10.3)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]59.1102.630
High resolution limit [Å]2.4602.460
Rpim0.0400.550
Number of reflections15793791
<I/σ(I)>14.31.3
Completeness [%]92.054.3
Redundancy66.3
CC(1/2)0.9980.570
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8.52770.2M NaF, 0.1 M bis-tris propane pH 8.5, 20% PEG3350

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