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6FVG

The Structure of CK2alpha with CCh507 bound

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04-1
Synchrotron siteDiamond
BeamlineI04-1
Temperature [K]100
Detector technologyPIXEL
Collection date2016-06-25
DetectorDECTRIS PILATUS 6M-F
Wavelength(s)0.92818
Spacegroup nameP 1 21 1
Unit cell lengths60.183, 45.931, 63.706
Unit cell angles90.00, 111.22, 90.00
Refinement procedure
Resolution56.100 - 1.600
R-factor0.208
Rwork0.206
R-free0.22900
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)5cu6
RMSD bond length0.010
RMSD bond angle0.920
Data reduction softwareDIALS
Data scaling softwareAimless (0.5.26)
Phasing softwarePHASER
Refinement softwareBUSTER (2.10.3)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]56.10056.1001.640
High resolution limit [Å]1.6007.1601.600
Rmerge0.0490.0420.727
Rmeas0.0580.0490.866
Rpim0.0310.0260.466
Number of reflections43028
<I/σ(I)>9.2
Completeness [%]99.999.699.8
Redundancy3.33.53.3
CC(1/2)0.9970.9920.745
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.5298112.5mM Mes pH 6.5, 35% glycerol ethoxylate, 180 mM ammonium acetate

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