6FS2
MCL1 in complex with indole acid ligand
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-02-09 |
| Detector | RIGAKU SATURN 944 |
| Wavelength(s) | 1.54 |
| Spacegroup name | P 1 |
| Unit cell lengths | 46.710, 46.710, 47.493 |
| Unit cell angles | 74.74, 74.74, 61.83 |
Refinement procedure
| Resolution | 45.200 - 2.550 |
| R-factor | 0.192 |
| Rwork | 0.186 |
| R-free | 0.25400 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.050 |
| Data reduction software | iMOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.6) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.220 | 2.750 |
| High resolution limit [Å] | 2.550 | 2.550 |
| Number of reflections | 10721 | |
| <I/σ(I)> | 8.55 | 2.05 |
| Completeness [%] | 97.2 | 96.1 |
| Redundancy | 2 | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | unknown |
