6FQH
GluA2(flop) S729C ligand binding core dimer bound to NBQX at 1.76 Angstrom resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-18 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | P 61 |
Unit cell lengths | 108.107, 108.107, 99.080 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 54.053 - 1.759 |
R-factor | 0.191023582719 |
Rwork | 0.189 |
R-free | 0.22398 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3kgc |
RMSD bond length | 0.011 |
RMSD bond angle | 1.172 |
Data reduction software | xia2 |
Data scaling software | Aimless (0.5.26) |
Phasing software | PHASER |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.053 | 1.790 |
High resolution limit [Å] | 1.759 | 1.760 |
Rmeas | 0.041 | |
Rpim | 0.016 | |
Number of reflections | 65151 | |
<I/σ(I)> | 23.1 | |
Completeness [%] | 100.0 | |
Redundancy | 6.7 | |
CC(1/2) | 1.000 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 289 | 0.1M tri-sodium Citrate, 20% PEG 3000 |