6FKO
Deoxyguanylosuccinate synthase (DgsS) quaternary structure with ATP, dGMP, hadacidin at 2.1 Angstrom resolution
Replaces: 6FJRExperimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-09 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.980097 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 91.970, 91.970, 192.750 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.710 - 2.100 |
R-factor | 0.191 |
Rwork | 0.189 |
R-free | 0.22200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.080 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.188 | 2.220 |
High resolution limit [Å] | 2.106 | 2.106 |
Number of reflections | 49180 | |
<I/σ(I)> | 8.4 | |
Completeness [%] | 99.5 | |
Redundancy | 5.91 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 291 | 0.2 M (NH4)2SO4 0.1 M Na3 Cit 5.6 pH 25 %w/v PEG 4K |