6FBE
KlenTaq DNA polymerase processing a modified primer - bearing the modification upstream at the third primer nucleotide.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-09-02 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 0.999990 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 108.480, 108.480, 90.309 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.973 - 1.589 |
R-factor | 0.1766 |
Rwork | 0.175 |
R-free | 0.20320 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.704 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.12rc1_2815: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.973 | 1.597 |
High resolution limit [Å] | 1.589 | 1.589 |
Rmeas | 0.108 | 1.404 |
Number of reflections | 159958 | 25710 |
<I/σ(I)> | 8.39 | 0.9 |
Completeness [%] | 99.8 | 99.3 |
Redundancy | 4.79 | 4.45 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 291 | 20 % PEG 4000, 0.1 M HEPES, 20 mM manganese(II) chloride, 0.1 M sodium acetate |