6F1C
C1rC1s complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04-1 |
| Synchrotron site | Diamond |
| Beamline | I04-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-01-31 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.92 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 96.779, 124.265, 195.499 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 97.749 - 4.200 |
| R-factor | 0.2499 |
| Rwork | 0.247 |
| R-free | 0.30500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4lor |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.907 |
| Data reduction software | xia2 |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX (dev_2722) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 97.800 | 4.700 |
| High resolution limit [Å] | 4.200 | 4.200 |
| Number of reflections | 17763 | |
| <I/σ(I)> | 6.6 | |
| Completeness [%] | 99.8 | |
| Redundancy | 7.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | 12-18% PEG 8000, 100 mM Imidazole at pH 8.0 |
