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6EVF

Structure of E285D S. cerevisiae Fdc1 with prFMN in the hydroxylated form

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I02
Synchrotron siteDiamond
BeamlineI02
Temperature [K]100
Detector technologyPIXEL
Collection date2013-12-01
DetectorDECTRIS PILATUS 6M
Wavelength(s).979
Spacegroup nameP 1 21 1
Unit cell lengths114.100, 96.820, 116.780
Unit cell angles90.00, 96.61, 90.00
Refinement procedure
Resolution34.350 - 2.060
R-factor0.16965
Rwork0.167
R-free0.21273
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4zac
RMSD bond length0.016
RMSD bond angle1.821
Data reduction softwarexia2
Data scaling softwarexia2
Phasing softwareREFMAC
Refinement softwareREFMAC (5.8.0158)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]34.3503.134
High resolution limit [Å]2.0602.060
Rmeas1.071
Number of reflections15413815457
<I/σ(I)>8.35
Completeness [%]99.0
Redundancy2.92.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2770.1M sodium cacodylate pH 6.5, 0.25M Calcium Acetate, 15% PEG 4k

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