6EQZ
A MamC-MIC insertion in MBP scaffold at position K170
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-09-03 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.976 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 110.682, 113.813, 115.511 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.696 - 2.293 |
R-factor | 0.2082 |
Rwork | 0.205 |
R-free | 0.27380 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5e7u |
RMSD bond length | 0.009 |
RMSD bond angle | 1.193 |
Data scaling software | XDS |
Phasing software | REFMAC |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.700 | 2.350 |
High resolution limit [Å] | 2.290 | 2.290 |
Rmerge | 0.252 | 2.133 |
Number of reflections | 65839 | |
<I/σ(I)> | 5.5 | |
Completeness [%] | 99.6 | |
Redundancy | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 1,86 M Tris-Ammonium citrate |