6EOO

DPP8 - Apo, space group 20

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-08-03
Detector	DECTRIS PILATUS 6M-F
Wavelength(s)	0.91587
Spacegroup name	C 2 2 21
Unit cell lengths	162.835, 247.064, 260.849
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	44.650 - 2.500
R-factor	0.23033
Rwork	0.229
R-free	0.25350
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1orv
RMSD bond length	0.007
RMSD bond angle	1.115
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	REFMAC (5.8.0155)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.650	2.660
High resolution limit [Å]	2.500	2.500
Number of reflections	180252	30424
<I/σ(I)>	13.2	1.92
Completeness [%]	99.9	100
Redundancy	8.52	8.55
CC(1/2)		0.720

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277	Na Citrate 0.46M