6ENW
X-ray structure of Auoxo4-encapsulated horse spleen apoferritin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-09-14 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5418 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 180.878, 180.878, 180.878 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 104.430 - 2.600 |
R-factor | 0.186 |
Rwork | 0.184 |
R-free | 0.23600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5erk |
RMSD bond length | 0.013 |
RMSD bond angle | 1.474 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 104.430 | 2.640 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.187 | 0.414 |
Rpim | 0.145 | 0.404 |
Number of reflections | 8209 | |
<I/σ(I)> | 5.4 | |
Completeness [%] | 99.0 | |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.6-0.8 M (NH4)2SO4, 0.1 M Tris pH 7.4-7.7, 50-60 mM CdSO4 |