6EIR
DYRK1A in complex with XMD15-27-2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-09-19 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.984003 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 87.685, 87.493, 229.041 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.940 - 2.400 |
R-factor | 0.23487 |
Rwork | 0.234 |
R-free | 0.25813 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.122 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.410 |
Number of reflections | 66701 |
<I/σ(I)> | 12.97 |
Completeness [%] | 95.8 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M KSCN; 0.1 M NaCl; 10% PEG 3350, pH 6.8 |