6EHI
NucT from Helicobacter pylori
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-02-05 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97 |
Spacegroup name | P 1 |
Unit cell lengths | 61.350, 71.370, 110.470 |
Unit cell angles | 81.36, 74.30, 82.33 |
Refinement procedure
Resolution | 47.410 - 1.580 |
R-factor | 0.2035 |
Rwork | 0.201 |
R-free | 0.24630 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ggk |
RMSD bond length | 0.021 |
RMSD bond angle | 2.065 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.410 | 1.670 |
High resolution limit [Å] | 1.580 | 1.580 |
Rmeas | 0.070 | 0.595 |
Number of reflections | 227845 | 35428 |
<I/σ(I)> | 11.2 | 2.22 |
Completeness [%] | 93.0 | 89.5 |
Redundancy | 3.5 | 3.5 |
CC(1/2) | 0.997 | 0.859 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 291 | PEG 4000 28% Ammonium sulfate Sodium acetate pH 6 |