Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2011-11-27 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.7679 |
| Spacegroup name | P 3 |
| Unit cell lengths | 118.400, 118.400, 140.166 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 48.149 - 1.750 |
| R-factor | 0.1345 |
| Rwork | 0.134 |
| R-free | 0.16250 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4RMX |
| RMSD bond length | 0.009 |
| RMSD bond angle | 0.930 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | PHENIX ((dev_3092: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.850 |
| High resolution limit [Å] | 1.750 | 1.750 |
| Rmerge | 0.090 | 0.868 |
| Rmeas | 0.101 | 0.975 |
| Number of reflections | 443661 | 70838 |
| <I/σ(I)> | 15.16 | 1.8 |
| Completeness [%] | 99.7 | 98.3 |
| Redundancy | 5.1 | 4.8 |
| CC(1/2) | 0.999 | 0.685 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6 | 291 | 10% PEG 8000, 0.2M SrCl2, 0.1M MES pH 6.0 |
