6DWU
Crystal structure of complex of BBKI and Bovine Trypsin
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-11-12 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 1.000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 137.167, 483.880, 137.010 |
Unit cell angles | 90.00, 116.76, 90.00 |
Refinement procedure
Resolution | 49.230 - 3.960 |
R-factor | 0.2288 |
Rwork | 0.226 |
R-free | 0.28150 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 4.030 |
High resolution limit [Å] | 3.960 | 3.960 |
Rmeas | 0.153 | 0.346 |
Rpim | 0.070 | 0.201 |
Number of reflections | 124813 | 2619 |
<I/σ(I)> | 8.16 | 3.01 |
Completeness [%] | 88.7 | 37.3 |
Redundancy | 4 | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 17.5% PEG3350 |