6DTZ
Crystal structure of eukaryotic DNA primase large subunit iron-sulfur cluster domain, Y397F mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER X8 PROTEUM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-11-24 |
Detector | Bruker Platinum 135 |
Wavelength(s) | 1.542 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.806, 50.810, 90.035 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 22.120 - 1.360 |
R-factor | 0.157 |
Rwork | 0.155 |
R-free | 0.17900 |
Structure solution method | SAD |
Data reduction software | PROTEUM PLUS |
Data scaling software | PROTEUM PLUS |
Phasing software | SHELXDE |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.120 | 1.410 |
High resolution limit [Å] | 1.360 | 1.360 |
Rmerge | 0.046 | 0.328 |
Number of reflections | 40483 | 3945 |
<I/σ(I)> | 12.72 | 2.21 |
Completeness [%] | 98.7 | 97.87 |
Redundancy | 1.9 | 1.8 |
CC(1/2) | 0.796 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 289 | 100 mM TRIS, 40% MPD |