6DN8
SPRY domain-containing SOCS box protein 2 complexed with (GZJ)VDINNN(CY3) Cyclic peptide inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-06-16 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95370 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 49.020, 109.370, 118.100 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.270 - 1.750 |
R-factor | 0.194 |
Rwork | 0.193 |
R-free | 0.21000 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.040 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.270 | 1.840 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.081 | 0.822 |
Rpim | 0.030 | 0.295 |
Number of reflections | 64838 | |
<I/σ(I)> | 16.2 | 2.7 |
Completeness [%] | 99.9 | |
Redundancy | 8.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 277.15 | 0.2M NH4SO4, 0.1M NaAc, 25% PEG4,000 |