6DKJ
human GIPR ECD and Fab complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 90 |
Detector technology | PIXEL |
Collection date | 2015-09-11 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.907, 63.649, 159.099 |
Unit cell angles | 90.00, 92.56, 90.00 |
Refinement procedure
Resolution | 19.719 - 1.950 |
R-factor | 0.2005 |
Rwork | 0.199 |
R-free | 0.23840 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.12) |
Phasing software | PHASER |
Refinement software | PHENIX ((dev-2328_1692)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 19.740 | 19.740 | 1.990 |
High resolution limit [Å] | 1.950 | 9.940 | 1.950 |
Rmerge | 0.095 | 0.028 | 0.633 |
Rmeas | 0.111 | 0.033 | 0.737 |
Rpim | 0.057 | 0.017 | 0.375 |
Total number of observations | 294866 | ||
Number of reflections | 79376 | 563 | 4537 |
<I/σ(I)> | 9.7 | ||
Completeness [%] | 97.6 | 86.3 | 97.1 |
Redundancy | 3.7 | 3.6 | 3.8 |
CC(1/2) | 0.997 | 0.999 | 0.817 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 10% PEG 4000 and 20% isopropanol |