6DBZ
Crystal structure of Nudix 1 from Arabidopsis thaliana complexed with isopentenyl diphosphate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-01-25 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 36.050, 72.751, 116.390 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 61.691 - 1.900 |
R-factor | 0.1891 |
Rwork | 0.187 |
R-free | 0.22920 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.117 |
Data reduction software | MOSFLM (7.1.0) |
Data scaling software | Aimless (0.3.11) |
Phasing software | MOLREP (11.2.08) |
Refinement software | PHENIX ((1.12_2829)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 72.750 | 9.130 |
High resolution limit [Å] | 1.670 | 1.670 |
Rmerge | 0.100 | |
Number of reflections | 36756 | |
<I/σ(I)> | 12.7 | |
Completeness [%] | 100.0 | |
Redundancy | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 277 | 0.1 M succinic acid pH 5.0 20% PEG 4000 0.3 M magnesium nitrate |