6DA1

ETS1 in complex with synthetic SRR mimic

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08B1-1
Synchrotron site	CLSI
Beamline	08B1-1
Temperature [K]	100
Detector technology	CCD
Collection date	2017-10-03
Detector	MARMOSAIC 300 mm CCD
Wavelength(s)	0.97952
Spacegroup name	P 32 2 1
Unit cell lengths	75.330, 75.330, 115.331
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	56.783 - 2.000
R-factor	0.217423045467
Rwork	0.216
R-free	0.24780
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1md0
RMSD bond length	0.002
RMSD bond angle	0.441
Data reduction software	MOSFLM (7.2.2)
Data scaling software	Aimless (0.5.32)
Phasing software	PHASER (2.8.0)
Refinement software	PHENIX (1.12_2829)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	65.240	2.050
High resolution limit [Å]	2.000	2.000
Rmerge	0.133	1.898
Rmeas	0.094
Rpim	0.038	0.550
Number of reflections	26181
<I/σ(I)>	12.7
Completeness [%]	100.0
Redundancy	11.1
CC(1/2)	0.999	0.938

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.3	277.15	PEG 3350, lithium sulfate, ethylene glycol, MES