6D4F
Crystal structure of PTP epsilon D2 domain (A455N/V457Y/E597D)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | AREA DETECTOR |
Collection date | 2015-01-13 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 61.470, 73.489, 75.656 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.015 - 1.909 |
R-factor | 0.1926 |
Rwork | 0.190 |
R-free | 0.22500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2jjd |
RMSD bond length | 0.007 |
RMSD bond angle | 0.811 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_2376: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.940 |
High resolution limit [Å] | 1.909 | 1.910 |
Rmerge | 0.064 | 0.486 |
Number of reflections | 26610 | |
<I/σ(I)> | 28 | |
Completeness [%] | 97.4 | 71.8 |
Redundancy | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 292 | 0.1 M imidazole pH 8.0, 0.2 M calcium acetate hydrate, 20% (w/v) polyethylene glycol 1000 |