6D29
HLA-B*57:01 presenting TSMSFVPRPW
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-02-04 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9537 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.742, 81.917, 109.356 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.959 - 1.880 |
R-factor | 0.1904 |
Rwork | 0.189 |
R-free | 0.22150 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5t6y |
RMSD bond length | 0.004 |
RMSD bond angle | 0.861 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1690) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.980 |
High resolution limit [Å] | 1.880 | 1.880 |
Rmerge | 0.076 | 0.620 |
Number of reflections | 37733 | 5374 |
<I/σ(I)> | 17.5 | 3.5 |
Completeness [%] | 99.0 | 98 |
Redundancy | 5.6 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.4 | 294 | 18 % PEG 4000, 0.2 M ammonium acetate and 0.1 M tri-sodium citrate pH 5.4. |