6CLA
2.80 A MicroED structure of proteinase K at 6.0 e- / A^2
Experimental procedure
Collection date | 2016-03-07 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 67.450, 67.450, 100.818 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.010 - 2.800 |
R-factor | 0.26701 |
Rwork | 0.263 |
R-free | 0.32562 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 6cl7 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.678 |
Data reduction software | MOSFLM (7.1.0) |
Data scaling software | Aimless (0.5.32) |
Refinement software | REFMAC (5.8.0194) |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |