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6CJE

Crystal Structure of Mnk2-D228G in complex with Inhibitor

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 5.0.1
Synchrotron siteALS
Beamline5.0.1
Temperature [K]100
Detector technologyCCD
Collection date2012-04-06
DetectorADSC QUANTUM 315r
Wavelength(s)0.987
Spacegroup nameP 32 2 1
Unit cell lengths105.915, 105.915, 72.658
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution38.780 - 3.360
R-factor0.21629
Rwork0.212
R-free0.31573
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2hw7
RMSD bond length0.012
RMSD bond angle1.883
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwareREFMAC (5.6.0117)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]40.0003.440
High resolution limit [Å]3.3503.350
Number of reflections6977
<I/σ(I)>4
Completeness [%]98.0
Redundancy10.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.5300.1520-30% (w/v) polyacrylic acid 5100, 1-5% PEG 400, and 50 mM Hepes (pH 7.5)

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