6BYX
Complex structure of LOR107 mutant (R259N) with tetrasaccharide substrate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08B1-1 |
Synchrotron site | CLSI |
Beamline | 08B1-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-09-15 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 0.9787 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 83.050, 120.959, 127.221 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.890 - 2.208 |
R-factor | 0.2053 |
Rwork | 0.204 |
R-free | 0.25460 |
RMSD bond length | 0.008 |
RMSD bond angle | 0.933 |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13rc2_2981: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.890 | 2.260 |
High resolution limit [Å] | 2.210 | 2.210 |
Number of reflections | 64618 | |
<I/σ(I)> | 23.8 | |
Completeness [%] | 99.0 | |
Redundancy | 14.8 | |
CC(1/2) | 1.000 | 0.910 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 25.5% PEG8K, 0.17M Ammonium Sulfate, 0.1M Mes pH 6.5, 15% Glycerol |