6BHR
HIV-1 immature CTD-SP1 hexamer in complex with IP6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-07-03 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 1 |
Spacegroup name | P 6 |
Unit cell lengths | 70.939, 70.939, 42.041 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.469 - 2.908 |
R-factor | 0.2188 |
Rwork | 0.215 |
R-free | 0.26510 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5i4t |
RMSD bond length | 0.005 |
RMSD bond angle | 1.090 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.900 |
Number of reflections | 2665 |
<I/σ(I)> | 10.3 |
Completeness [%] | 96.3 |
Redundancy | 8.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 290 | 0.2 M NaCl 20% PEG 3350 0.1 M Bis-Tris pH 5.35 |