6B99
Hsp90-alpha N-domain bound to NECA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-05 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97946 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 64.547, 90.077, 98.409 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.891 - 1.602 |
R-factor | 0.165339757759 |
Rwork | 0.164 |
R-free | 0.18274 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1yer |
RMSD bond length | 0.006 |
RMSD bond angle | 1.032 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX (1.9_1692) |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.105 | 0.561 |
Number of reflections | 37663 | |
<I/σ(I)> | 26.6 | 2.8 |
Completeness [%] | 99.2 | 99.2 |
Redundancy | 6 | 5.2 |
CC(1/2) | 0.791 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.4 | 277 | Bis Tris Propane pH 6.4, MgCl2, PEG 2000 MME. Soak with NECA |