6B8O
WT Ig-like V Domain with Phosphatidylserine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2017-07-28 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.00001 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 160.331, 160.331, 86.205 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.360 - 2.200 |
R-factor | 0.2236 |
Rwork | 0.222 |
R-free | 0.26060 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ud7 |
RMSD bond length | 0.019 |
RMSD bond angle | 2.165 |
Data scaling software | Aimless (0.5.32) |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 47.360 | 47.360 | 2.260 |
High resolution limit [Å] | 2.200 | 9.590 | 2.200 |
Rmerge | 0.106 | 0.034 | 1.733 |
Total number of observations | 752391 | 8284 | 59146 |
Number of reflections | 57469 | 807 | 4402 |
<I/σ(I)> | 19.8 | 64 | 1.8 |
Completeness [%] | 100.0 | 99.3 | 100 |
Redundancy | 13.1 | 10.3 | 13.4 |
CC(1/2) | 0.999 | 1.000 | 0.579 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 0.2 M NaI, 1.6 M ammonium sulfate, 50 mM Tris 8.5 |