6B5Q
DCN1 bound to 38
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-10-09 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.9787 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 88.087, 90.841, 105.010 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 16.440 - 2.160 |
R-factor | 0.197 |
Rwork | 0.195 |
R-free | 0.24100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 0.990 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.200 |
High resolution limit [Å] | 2.160 | 5.860 | 2.160 |
Rmerge | 0.048 | 0.028 | 0.226 |
Rmeas | 0.052 | 0.031 | 0.244 |
Rpim | 0.019 | 0.012 | 0.090 |
Total number of observations | 168961 | ||
Number of reflections | 22799 | 1197 | 1113 |
<I/σ(I)> | 15.5 | ||
Completeness [%] | 99.8 | 96.5 | 100 |
Redundancy | 7.4 | 6.6 | 7.3 |
CC(1/2) | 0.999 | 0.981 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 37 % PEG 300, 0.1 M phosphate-citrate pH 4.2 |