6B0B
Crystal structure of human APOBEC3H
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-08-23 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.28 |
Spacegroup name | P 31 1 2 |
Unit cell lengths | 101.293, 101.293, 211.217 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.250 - 3.280 |
R-factor | 0.353353535773 |
Rwork | 0.353 |
R-free | 0.36244 |
Structure solution method | SAD |
RMSD bond length | 0.002 |
RMSD bond angle | 0.574 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHELXD |
Refinement software | PHENIX (dev_2926) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.300 | 3.480 |
High resolution limit [Å] | 3.280 | 3.280 |
Rmerge | 0.210 | 3.200 |
Rpim | 0.048 | |
Number of reflections | 366518 | 37356 |
<I/σ(I)> | 13.4 | 0.7 |
Completeness [%] | 98.3 | 89 |
Redundancy | 20.4 | 21.1 |
CC(1/2) | 0.999 | 0.500 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | NH4I, PEG3350 |