6AOZ
Crystal structure of human FLASH N-terminal domain C54S/C83A (Crystal form 1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-11-12 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9792 |
Spacegroup name | P 1 |
Unit cell lengths | 39.281, 41.086, 60.951 |
Unit cell angles | 95.58, 105.18, 113.40 |
Refinement procedure
Resolution | 36.721 - 2.100 |
R-factor | 0.2175 |
Rwork | 0.215 |
R-free | 0.25410 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ano |
RMSD bond length | 0.003 |
RMSD bond angle | 0.405 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.721 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.428 | 0.428 |
Rpim | 0.278 | |
Number of reflections | 18642 | 1888 |
<I/σ(I)> | 18.2 | 3.25 |
Completeness [%] | 97.9 | 97.7 |
Redundancy | 3.9 | 3.4 |
CC(1/2) | 0.822 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 4% (w/v) tacsimate pH 7.0, 11 % (w/v) PEG 3350 |