6AO0
CAT192 Fab Insertion Mutant H2/L2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-03-03 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.5419 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 109.060, 86.590, 45.890 |
Unit cell angles | 90.00, 100.57, 90.00 |
Refinement procedure
Resolution | 31.237 - 2.350 |
R-factor | 0.2082 |
Rwork | 0.206 |
R-free | 0.26100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6amj |
RMSD bond length | 0.002 |
RMSD bond angle | 0.483 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 31.237 | 2.480 |
High resolution limit [Å] | 2.350 | 2.350 |
Rmerge | 0.332 | |
Number of reflections | 16303 | 7335 |
<I/σ(I)> | 2.9 | |
Completeness [%] | 85.1 | |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 277 | 2M Ammonium sulfate, 0.1M sodium acetate trihydrate pH 4.6 |