6AIT
Crystal structure of E. coli BepA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL32XU |
Synchrotron site | SPring-8 |
Beamline | BL32XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-11-16 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 |
Unit cell lengths | 85.844, 104.674, 104.971 |
Unit cell angles | 113.61, 105.84, 104.03 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.595 | 2.691 |
High resolution limit [Å] | 2.598 | 2.598 |
Rmerge | 0.104 | 1.218 |
Rmeas | 0.122 | 1.434 |
Rpim | 0.063 | 0.748 |
Number of reflections | 89522 | 8738 |
<I/σ(I)> | 8.88 | |
Completeness [%] | 98.2 | 94.9 |
Redundancy | 3.7 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 | 2 M ammonium sulfate |