6A1Z
Crystal Structure of dimeric Kinesin-3 KIF13B
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-12-30 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9789 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 87.380, 87.380, 97.490 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.869 - 2.580 |
R-factor | 0.2401 |
Rwork | 0.238 |
R-free | 0.28640 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5zbr |
RMSD bond length | 0.009 |
RMSD bond angle | 1.119 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.870 | 2.650 |
High resolution limit [Å] | 2.580 | 2.580 |
Rmerge | 0.062 | 0.665 |
Number of reflections | 13889 | 1023 |
<I/σ(I)> | 14 | |
Completeness [%] | 99.4 | |
Redundancy | 18.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 6.9 | 289 | 1.4M Na/KPO4 |