Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-10-11 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.9999 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 91.613, 63.570, 80.095 |
| Unit cell angles | 90.00, 118.39, 90.00 |
Refinement procedure
| Resolution | 45.530 - 1.700 |
| R-factor | 0.171 |
| Rwork | 0.170 |
| R-free | 0.19930 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1z57 |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.736 |
| Data reduction software | XDS |
| Data scaling software | Aimless (0.7.4) |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 45.530 | 45.530 | 1.730 |
| High resolution limit [Å] | 1.700 | 9.000 | 1.700 |
| Rmerge | 0.065 | 0.034 | 0.450 |
| Rmeas | 0.075 | 0.039 | 0.528 |
| Rpim | 0.037 | 0.020 | 0.271 |
| Total number of observations | 172609 | 1238 | 7870 |
| Number of reflections | 44218 | 327 | 2200 |
| <I/σ(I)> | 11.1 | 27 | 2.4 |
| Completeness [%] | 99.2 | 99 | 93.8 |
| Redundancy | 3.9 | 3.8 | 3.6 |
| CC(1/2) | 0.997 | 0.998 | 0.839 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 9 | 277 | 14% PEG 6k, 0.1M bicine |
