6XWH
Crystal Structure of the Human RXR DNA-Binding Domain Homodimer Bound to the Human Hoxb13 DR0 Response Element
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-09-21 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.984 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 45.705, 62.522, 53.635 |
Unit cell angles | 90.00, 104.84, 90.00 |
Refinement procedure
Resolution | 22.220 - 2.100 |
R-factor | 0.187 |
Rwork | 0.185 |
R-free | 0.22400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4cn5 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.040 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.5.1) |
Refinement software | BUSTER |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 22.220 | 22.220 | 2.230 |
High resolution limit [Å] | 2.100 | 6.260 | 2.100 |
Rmerge | 0.046 | 0.028 | 11.082 |
Rmeas | 0.056 | 0.034 | 14.112 |
Total number of observations | 46744 | ||
Number of reflections | 15542 | 668 | 1632 |
<I/σ(I)> | 9.21 | 35.44 | 0.06 |
Completeness [%] | 90.5 | 98.2 | 59.2 |
Redundancy | 3.008 | 3.06 | 2.053 |
CC(1/2) | 0.998 | 0.997 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20% PEG 3350, 0.15 M di-sodium DL-malonate |