6XP6

3C11-DQ2-glia-a2 complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX2
Synchrotron site	Australian Synchrotron
Beamline	MX2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-03-20
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.95372
Spacegroup name	P 21 21 21
Unit cell lengths	91.847, 143.047, 170.153
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.030 - 2.400
R-factor	0.177
Rwork	0.176
R-free	0.21240
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5jo4 6mfg
RMSD bond length	0.006
RMSD bond angle	0.831
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.030	2.486
High resolution limit [Å]	2.400	2.400
Rpim	0.072	0.556
Number of reflections	88213	8724
<I/σ(I)>	8.78
Completeness [%]	99.9
Redundancy	2
CC(1/2)	0.993	0.633

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293.15	10% PEG 4000 20% 2-propanol 0.1M HEPES