6W0Q
APE1 endonuclease product complex D148E
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-03-31 |
Detector | DECTRIS PILATUS 200K |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 |
Unit cell lengths | 44.435, 60.496, 72.982 |
Unit cell angles | 83.51, 79.62, 88.61 |
Refinement procedure
Resolution | 24.810 - 1.890 |
R-factor | 0.1872 |
Rwork | 0.186 |
R-free | 0.22290 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5dff |
RMSD bond length | 0.009 |
RMSD bond angle | 1.025 |
Data reduction software | PHENIX (1.17.1_3660) |
Data scaling software | HKL-3000 |
Phasing software | PHENIX (1.17.1_3660) |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.810 | 1.930 |
High resolution limit [Å] | 1.890 | 1.900 |
Rmeas | 0.087 | 0.545 |
Number of reflections | 111259 | 5232 |
<I/σ(I)> | 18 | 2.3 |
Completeness [%] | 99.8 | |
Redundancy | 4.1 | |
CC(1/2) | 0.773 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 291 | 10% PEG20000, 100 mM sodium citrate, pH 5.0, and 200 mM MgCl2 |